Pre-configured System

Atlas HD Reaction Calorimeter

An easy-to-use, high-performance calorimetry system. Using either Heat Flow Calorimetry (HFC) or Power Compensation Calorimetry (PCC), it can generate power and enthalpy graphs quickly and easily.

At a glance

The Atlas HD Reaction Calorimeter operates in either Heat Flow Calorimetry (HFC) or Power Compensation Calorimetry (PCC) mode.  The system is designed for ease of use with the generation of power and enthalpy graphs made simple and quick.

In addition, the simple configuration of reaction temperatures, dosing quantities, and alarms, provides you with a safe and accurate reaction calorimetry system and offers great value for calorimetry chemists.

Discover more about reaction calorimetry here.

  • Designed for ease of use
  • Safe & accurate reaction calorimetry system
  • Simple & quick power & enthalpy graph generation

1. HFC and PCC measurements

The system offers two modes; Heat Flow Calorimetry (HFC) or Power Compensation Calorimetry (PCC), allowing you to choose which mode is suitable for your process.  HFC is generally used for reactions where the heater may have an effect on the chemistry since the dip in heater is not used during the reaction. HFC is also preferred when large exotherms are expected. PCC is used where quicker results are required, since no pre- and post-calibration is required. All important reaction parameters can be monitored in real-time using the Atlas HD Calorimeter.

Syrris Atlas HD Calorimetry System, chemist using software

2. Powerful automation

The Atlas PC Reaction Calorimetry Software offers truly easy reaction calorimetry operation. Configuration of parameters such as reaction temperature, dosing quantities, expected power level (e.g. moderate endotherm; strong exotherm), and alarms (with subsequent actions) are defined in an easy to use wizard.  Everything is controlled automatically during the experiment including stabilization at desired reaction temperature, reagent addition and in the case of HFC, pre- and/or post-run calibration. No user intervention is required during the entire process.

Syrris Atlas HD Calorimetry System Touchscreen

3. Flexible

The Atlas HD Reaction Calorimeter is destined to be a very popular addition to your laboratory.  Easy to set and configure, reaction calorimetry cannot be made simpler.  A wide range of vacuum jacketed reactors from 100 mL to 2 L and the ability to perform HFC or PCC gives you choice.  When there are no reaction calorimetry experiments to perform, the system will operate seamlessly as an automated jacketed reactor.

A photograph of 2 Syrris Atlas HD automated chemistry reactors with different size vessels

4. Quick and easy data analysis

The software automatically includes the calibration, compensates for the enthalpy of addition and deviations from isothermal conditions. Post experiment analysis is made easy by the Atlas Reporting Software featuring “single click” plotting of power and enthalpy.

Syrris Atlas HD Computer Screen Reaction Calorimetry

What our customers say

We purchased the Atlas Calorimeter as it has the capability to perform both Heat Flow Calorimetry and Power Compensation Calorimetry, making it a really good addition to the laboratory.”

Dr. Deepak Jain, Head of Process R&D, Pfizer
Dr. Deepak Jain, Head of Process R&D, Pfizer

Specifications

Vessel Volume Range 50 mL, 100 mL, 250 mL, 500 mL, 1 L, 2 L (DN80), 1 L, 2 L, and 5 L (DN150)
Vessel Shapes Torispherical, Conical, Round Bottom
Vessel Profiles Jacketed, Vacuum Jacketed
Other Vessel Types No (Round Bottom Flasks Available with Regular Atlas Base)
Temperature Range -90°C to 250°C (with suitable seal kit)
Stirring Options Scorpion Overhead Stirrer (up to 800rpm/11Ncm torque), High Speed Available, High Torque Available
Automation Yes – as standard
Modes of Operation Atlas HD Touch Screen Control, Atlas PC Software, Manual Operation
Sensor Options Temperature, pH, Pressure, Turbidity, In-situ FTIR, Other Sensors Available
Pressure Range Vacuum (50mbar) to 0.5 Bar, See Atlas 200 Bar Pressure Systems for High Pressure up to 200 Bar, See Atlas 3 Bar Pressure Systems for High Pressure up to 3 Bar
Reaction Calorimetry Heat Flow Calorimetry (HFC), Power Compensation Calorimetry (PCC)
Reagent Addition and Sampling Manual Dosing, Automated Dosing (Volumetric), Automated Dosing (Gravimetric), Sampling of Liquids, Full Gas Control, Atlas Syringe Pump Range
Syrris Atlas HD Calorimetry System close-up
A photograph of the Atlas Scorpion Overhead Stirrer Motor
Syrris Atlas HD Automated Jacketed reactor, close-up of touchscreen
Syrris Atlas HD Syringe Pump close-up

What we say

Atlas HD is the perfect product for those wanting an easy to use setup that generates highly accurate data.

Leandro Nogueira, Regional Director Europe & Latin America
Leandro Nogueira - Regional Sales Director for Syrris

Modules

  1. Base units

    • Atlas HD Potassium

      (included)

      The Atlas HD Potassium is the base reactor system on which all Atlas HD systems are built, and can be […]

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  2. Automation

    • Atlas PC Software 1

      (included)

      Atlas Software 1 is an easy-to-use PC based application for control and analysis of experiments. Whole systems including stirrers, circulators, […]

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    • Atlas Reporting Software

      (included)

      The Atlas Reporting Software allows easy graphical analysis of log files generated by either the Base Unit, Atlas Software 1, […]

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  3. Advanced Applications

    • Atlas Calorimetry Upgrade Kit

      (included)

      The Atlas HD Calorimetry Upgrade Kit includes all the necessary parts to upgrade the Atlas HD Potassium base system to […]

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  4. Circulation

    • Circulator and Fluid

      (optional)

      Circulator options from industry-leading manufacturer, Huber. A range of circulator accessories and oils for whatever your application are available.

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  5. Dosing

  6. Optional modules

    • Atlas Syringe Pump

      (optional)

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    • Circulator and Fluid

      (optional)

      Circulator options from industry-leading manufacturer, Huber. A range of circulator accessories and oils for whatever your application are available.

      View module details

Support

These support articles may be helpful for this system